Investigation of slow dynamic processes in amorphous and crystalline polymers by 1D-MAS NMR spectroscopy [Elektronische Ressource] / von Ovidiu F. Pascui

Investigation of slow dynamic processesin amorphous and crystalline polymers by 1D-MAS NMR spectroscopyDissertationzur Erlangung des akademischen Grades doktor rerum naturalium (Dr. rer. nat.)vorgelegt derMathematisch-Naturwissenschaftlich-Technischen Fakultät(mathematisch-naturwissenschaftlicher Bereich)der Martin-Luther-Universität Halle-Wittenbergvon Herrn Ovidiu F. Pascuigeb. am: 29.8.1976 in Oradea, RumänienGutachter:1. Priv.-Doz. Dr. D. Reichert2. Prof. T. J. Bonagamba3. Prof. D. E. DemcoHalle(Saale)den 5 Februar 2003urn:nbn:de:gbv:3-000004823[ http://nbn-resolving.de/urn/resolver.pl?urn=nbn%3Ade%3Agbv%3A3-000004823 ]Summary: pageIntroduction........................................................................................................................................11. Short review of other methods than NMR, used to investigate polymer dynamics.......................32. 2D and 1D-MAS exchange experiments in NMR spectroscopy....................................................92.1 A simple NMR-MAS experiment........................................................................................92.2 2D-MAS NMR exchange .................................................................................................152.3 1D-MAS NMR exchange .................................................................................................222.3.1 ODESSA......................................................................................